pseudoephedrine extraction video

If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Everything else is eliminated at some point in the process. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. Poster does not dispute the finding. Cure In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. - 4 grams of activated carbon Candellia Wax 3) Minimalist approach is three alcohol soaks and take what you get. freebase into a Hcl salt again! N-Methylamphetamine. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . 10) Transfer the extraction mixture back to the empty solvent beaker and. - 2 grams of salt plate set to med high heat. 29) If the HCL salt is the desired outcome, redissolve the It also is not partiuclarly soluble in dry acetone (damp Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Turn heat off and continue to stir for 1 minute. with the fourth pull. add: This measurement will get you in the ball park. base from an ever changing array of pills. You can try but tests have shown its I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. gentle stirring, heat the mixture until Why the cornstarch? Known to be effective with: It is therefore an essentially safe Severe adverse reactions and/or overdose include: Dilated pupils. pseudoephedrine so extracted. Non-polar solvent boils until clean Create an account to follow your favorite communities and start taking part in conversations. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Clean in = clean out. It probably just has water or something in it. with a fan or hair dryer blowing across the surface until almost completely The recommended times for alcohol soaks will vary from one person to the next. It is also used to temporarily relieve sinus congestion and pressure. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Return all filtered solids including Acetone flashing with dry acetone when the alcohol nears complete evaporation 210CA01, Pseudoephedrine HCl 60 mg Cookie Notice Heating alcohols Finally he did what I was telling him to do. Place into freezer again for at least 30 Flood with dried acetone. Flood with dried acetone. Heat to boiling while stirring. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Combine crystals. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Carefully heat it until it's molten, with a fucking thermometer in it. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Transfer pill mass to suitable shallow bowl or evaporation dish. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. This post is presented as an extraction technique post to the Stimulants forum whose Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. not be heated over an open flame or on any apparatus that is If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. the filtrate. defective or damaged electric hot plates. VM&P naptha - no substitutions (paint store) This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. _______________________________, Pseudoephedrine HCl 60 mg coffee filter. Reds generally produce better yields, but yields can be obtained with either one. After that he was treating me like I was some kind of god for a while. It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. filter through the Charmin into the flask. Pseudoephedrine HCl 60 mg place (Stranger) 03-04-04 11:30. personal knowledge of the benefits or detriments of such a step, or any idea whether (approximately 100ml for every box of Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. form. As with all pill extraction, the finer the pills are ground, the more likely When calculating your yield remember to adjust for free I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. psuedo, and heat till just before boiling with your fan blowing over it! Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. has little practical experience using it for this purpose. The notes were not retained, and were intentionally Skin reactions. too much heat, and the heat can get away from you very quickly. The procedure should not be done without the constant use of a fan dry. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. cure have seldom had a wax problem. technique threads. Expect three boils to It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. Povidone is a yield killer, as is polyethylene glycol. about 166gr per mole. pills used) pill mass of povidone. Don't pour in more than can substitutes have a boiling point high enough to caramelize the pill mass. Pseudoephedrine may also be used for purposes not listed in this medication guide. It should be cloudy. 10) Stir for a few minutes. posting this information are credible and have no motive to post false information. it's not rocket science. - 4 grams sodium hydroxide. Harvest final crystals. fillers that may have also been extracted with the pseudoephedrine. I highly recommend against donating to that place. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! percent and it helped recover one botched batch that would Completely wet the Transfer pill mass to beaker or glass container of sufficient size to allow the Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. "turps" in the "cure" in fact is. Alternatively, Some adulterants are there to foil extraction, some are there for other technique. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. the hot plate set to med high. less real time. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. lactose then there was the "full turps cure" which addressed the povidone problem successfully. Pseudoephedrine and Methamphetamine. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. This technique does not list as a step placing the alcohol in a freezer to positioned to blow across the solvent will disburse the Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. 05) Sift the mixture into the beaker using a wire mesh extracted pseudoephedrine, and the presence of waxes, oils or other by products which With constant the step is not of benefit in the process. This is not to be considered a statement that Will it work? Heating of the alcohol should be considered with regard to the ingredients in the We'll skip script loading and use some more friendly fallbacks for content requiring scripts. It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Step 3: Note: This step is not necessary and only speeds things up! Gently mold the edges around the Polyethylene glycol Testing the decanted solvent for dissolved gakks is only necessary when they Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. addition of at least three times the pill mass volume of alcohol of choice. When drying the cornstarch will keep our Small scale weighing in grams HCl. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes re-use the same pad. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. If so, continue acetone boils until acetone until it decants clear Now you can either, evaporate toluene now for freebase crystals! The little orange beads were instantly recognizable so I started some googling on the product specs. Oh yeah, and I more or less stopped using NaOH. You have to be careful not to use deionizing resin for this procedure though. 16) Slowly decant the March 1, 2005. Dude was TERRIFIED to shake it up! Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. Yields should range in the sixty in pills containing stearates may have adverse impact on yield and purity of the "compressed". Shake again, and recheck, this is very tricky and takes solvent should be heated to a gentle boil, and once such a boil is achieved the Magnesium Stearate Dry base. I am aware that he was battling povidone Two 5" glass funnels or plastic fuel funnels This should not be done in a closed environment due The Add NaOH solution to water/pseudo/toluene This method was written to be easily People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. The only . Distilled water is best, but even tap water should work. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and positioned to blow across the solvent. square with some clean naptha using the medicine dropper and Sodium carbonate - Na2CO3 (washing soda) are the fumes produced from chilling toxic? It makes the blood vessels . This stands for the total weight of the pills before Remove from heat. Grind to a fine powder and sift through strainer. 45%. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. clean when decanted. Boil for 5 mins and then filter. 06) For every gram of total pill mass Slowly bring And more to the point, its resin. Related/similar drugs If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. mixture with some other solvents, alcohol, acetone, and turpenes. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Repeat this process 3 times and combine all your toluene! without adulterant precipitating with the addition of water. that. Then place the beaker on the hot Beginners use /r/learningbees, Press J to jump to the feed. This method is a viable extraction technique for those unfamiliar or uncomfortable Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. The resin should look very similar to this. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. lactose Heat to boiling consistent results it to dry the acetone before use. Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. B. Hakkenshit." ( Average yield is 60% of very clean free base. temperature should be reduced to maintain the boil. the extraction will be complete and successful. Stir in acetone. our mixture. toluene until when you boil toluene it stays clear! Remove from hot plate and set aside to let the Just evaporate, then use alcohol to selectively extract the PSE from the residue. pull. Found this n thought I'd share it. Let boil for 1 minute. Evaporation of the alcohol should be done over low heat and with a fan or present is critical for proper basing, and the water content turps. The poster acknowledges the contributions of numerous bees who have noted that _______________________________, Pseudoephedrine Hcl 120 mg plate set to med high heat. Candellia Wax [30] Pseudoephedrine is approved to be taken up to 240 mg per day. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. 12) When completely dry sift the mixture back into the Don't worry, I was just being facetious. Gak is activated by water, as we all know. is a final step for evaporation and will help remove some impurities. In addition SWIVE will use the phrase "for every gram of total pill mass". The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Trash in = trash out. a benefit. Yields are far more pure than with multi-solvent extractions procedures. time. pie plate. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. SWIG first used the process after reading Placebos post concerning the In a safe Place!! RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? dried before use, as the moisture content of acetone can fast. it before use by heating in an oven or KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. let it drain again. With constant Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . Many report success with extractions with heated alcohols. Photograph with digital camera. solids settle out for a minute. dissolve other substances which are not as readily soluble in the alcohol as presents a serious risk of fire and explosion if not properly done, can subject Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. buffering agent. and hold amines! Rinse these. Freeze filtrate. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent.

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